浩瀚色譜（山東）應用技術(shù)開發(fā)有限公司，建立了一種快速測定聚合級乙烯和丙烯中痕量CO,CH4,CO2含量的方法,驗證了該方法的線性范圍和檢測限,考察了該方法的精密度和回收率,并對乙烯和丙烯實際試樣中痕量CO,CH4,CO2的含量進行了分析.定量分析結(jié)果表明,在測試濃度范圍內(nèi),CO,CO2,CH4的峰面積與含量具有良好的線性關(guān)系,線性相關(guān)系數(shù)均大于0.990;回收率在93.90％～101.89％之間,5次重復測定結(jié)果的相對標準偏差均小于2％,定量結(jié)果準確可靠;CO,CH4,CO2的最低檢測限分別為31,14,12 μL/m3,滿足烯烴生產(chǎn)企業(yè)對烯烴產(chǎn)品質(zhì)量控制的需要.該方法為烯烴生產(chǎn)企業(yè)的烯烴產(chǎn)品質(zhì)量控制提供了一種新的高靈敏的分析方法.
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名稱：便攜式甲烷轉(zhuǎn)化爐
型號：HH-CH4-GC
適合于：安捷倫4890. 5890, 6890, 7890, 7820, 8860, 8890氣相色譜儀上；島津2010,2014,2030
HH-CH4-GC甲烷轉(zhuǎn)化爐的轉(zhuǎn)化效率高，安裝簡單，便攜式，小巧玲瓏，集成加熱，氣路，進樣，溫控，柱分離系統(tǒng)于一體；可擴展為二維/多維，反吹，切割系統(tǒng)。
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Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. has established a rapid method for determining trace amounts of CO, CH4, and CO2 in polymer grade ethylene and propylene. The linear range and detection limit of the method have been verified, and the precision and recovery rate of the method have been investigated. The content of trace amounts of CO, CH4, and CO2 in actual samples of ethylene and propylene has been analyzed. The quantitative analysis results show that within the test concentration range, CO, CO2, The peak area and content of CH4 have a good linear relationship, with linear correlation coefficients greater than 0.990; The recovery rate is between 93.90% and 101.89%, and the relative standard deviation of the five repeated determination results is less than 2%, indicating accurate and reliable quantitative results; The minimum detection limits for CO, CH4, and CO2 are 31, 14, and 12, respectively μ L/m3 meets the needs of olefin production enterprises for quality control of olefin products. This method provides a new and highly sensitive analytical method for olefin product quality control in olefin production enterprises
Name: Portable methane conversion furnace
Model: HH-CH4-GC
Suitable for: Agilent 4890, 5890, 6890, 7890, 7820, 8860, 8890 gas chromatographs; Shimadzu 201020142030
The HH-CH4-GC methane conversion furnace has high conversion efficiency, simple installation, portability, and is small and exquisite. It integrates heating, gas path, injection, temperature control, and column separation systems; Can be extended to 2D/multi-dimensional, blow back, cutting systems.
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