六氯乙硅烷制備途徑有兩種，其一是通過(guò)硅、氫氣和四氯化硅在某種溫度下反應(yīng)，產(chǎn)生含有六氯乙硅烷的混合氣體，再通過(guò)分離和提純得到六氯乙硅烷；其二是在改良西門子法生產(chǎn)多晶硅的過(guò)程中，冷氫化反應(yīng)的副產(chǎn)物中含有較多的六氯乙硅烷，可通過(guò)適當(dāng)?shù)姆蛛x提純得到六氯乙硅烷。
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名稱：DC-550不銹鋼填充柱
規(guī)格：3m*Φ3
*高使用溫度：240°C
貨號(hào)：20231119001
應(yīng)用：YS/T 1434-2021六氯乙硅烷組分含量的測(cè)定 氣相色譜法
GB/T 42720-2023電子特氣 六氯乙硅烷
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浩瀚色譜（山東）應(yīng)用技術(shù)開發(fā)有限公司，采用GC-TCD氣相色譜儀，熱導(dǎo)檢測(cè)器，面積歸一法測(cè)定六氯乙硅烷中三氯氫硅、四氯化硅、六氯乙硅烷及其他組分含量，結(jié)果滿意。
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There are two ways to prepare hexachloroethane. One is through the reaction of silicon, hydrogen gas, and tetrachlorosilane at a certain temperature to produce a mixed gas containing hexachloroethane, which is then separated and purified to obtain hexachloroethane; The second is that in the process of producing polycrystalline silicon using the improved Siemens method, the byproducts of the cold hydrogenation reaction contain a large amount of hexachloroethane, which can be obtained through appropriate separation and purification.
Name: DC-550 stainless steel filled column
Specification: 3m* Φ three
*High operating temperature: 240 ° C
Article number: 20231119001
Application: YS/T 1434-2021 Determination of Hexachloroethane Component Content Gas Chromatography
GB/T 42720-2023 Electronic Special Gas Hexachloroethane
Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. used a GC-TCD gas chromatograph, thermal conductivity detector, and area normalization method to determine the content of trichlorosilane, tetrachlorosilane, hexachloroethane, and other components in hexachloroethane, with satisfactory results.
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