照氣相色譜法測定（通則0521）測定。
色譜條件與系統(tǒng)適用性試驗 用聚苯乙烯-二乙烯基苯為固定相（PLOT Q型或極性相近）的毛細(xì)管柱；氫氣為載氣；柱溫90℃；進(jìn)樣口溫度為130℃；檢測器為熱導(dǎo)檢測器，溫度為130℃。取含有甲醇（0.01%）和二甲醚的混合標(biāo)準(zhǔn)氣，由氣體進(jìn)樣閥注入氣相色譜儀，記錄色譜圖。理論板數(shù)按二甲醚峰計算應(yīng)不低于1500，二甲醚峰與甲醇峰的分離度應(yīng)符合要求。
測定法 取本品，連接減壓閥，用銅管將減壓閥和氣體進(jìn)樣閥相連接，打開鋼瓶減壓閥，沖洗連接管道與各閥，調(diào)節(jié)流速使進(jìn)樣閥后的氣流以能在水中連續(xù)冒出氣泡為宜，設(shè)置氣體自動進(jìn)樣閥0.01分鐘時打開，1分鐘時關(guān)閉，記錄色譜圖。按面積歸一化法計算，即得。
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名稱：毛細(xì)管柱
固定相：聚苯乙烯-二乙烯基苯為固定相
規(guī)格：30m*0.53mm*40um
型號：HH-PLOT Q
應(yīng)用：藥典二甲醚
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Determine according to the gas chromatography method (General Rule 0521).
A capillary column with polystyrene divinylbenzene as the stationary phase (PLOT Q-type or similar polarity) for chromatographic conditions and system suitability testing; Hydrogen is the carrier gas; Column temperature 90 ℃; The inlet temperature is 130 ℃; The detector is a thermal conductivity detector with a temperature of 130 ℃. Take a mixed standard gas containing methanol (0.01%) and dimethyl ether, inject it into the gas chromatograph through the gas injection valve, and record the chromatogram. The number of theoretical plates calculated based on the dimethyl ether peak should not be less than 1500, and the separation degree between the dimethyl ether peak and the methanol peak should meet the requirements.
Determination method: Take this product, connect the pressure reducing valve, connect the pressure reducing valve and gas injection valve with a copper tube, open the pressure reducing valve of the steel cylinder, flush the connecting pipeline and each valve, adjust the flow rate to ensure that the airflow after the injection valve can continuously emit bubbles in water. Set the automatic gas injection valve to open at 0.01 minutes and close at 1 minute, and record the chromatogram. Calculate using the area normalization method to obtain.
Name: Capillary Column
Fixed phase: polystyrene divinylbenzene as the fixed phase
Specification: 30m * 0.53mm * 40um
Model: HH-PLOT Q
Application: Pharmacopoeia dimethyl ether
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