改進(jìn)明膠空心膠囊中殘留氯乙醇和環(huán)氧乙烷的測(cè)定方法。浩瀚色譜(山東)應(yīng)用技術(shù)開(kāi)發(fā)有限公司采用的10%聚乙二醇填充柱,檢測(cè)器采用FID和ECD,分別進(jìn)行測(cè)定。結(jié)果對(duì)氯乙醇和環(huán)氧乙烷的測(cè)定中,固定液為10%聚乙二醇填充柱;檢測(cè)器采用FID優(yōu)于ECD。結(jié)論該方法重現(xiàn)性佳,分離效果好。
名稱(chēng):填充柱
規(guī)格:2m*4mm,60-80目
型號(hào):聚乙二醇填充柱/6201釉化擔(dān)體
編號(hào):20230510002
*高溫度:240°C
Improve the determination method for residual chloroethanol and ethylene oxide in gelatin hollow capsules. Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. uses a 10% polyethylene glycol packed column, and the detector uses FID and ECD for separate measurements. In the determination of chloroethanol and ethylene oxide, the fixed solution was a 10% polyethylene glycol filled column; The detector uses FID better than ECD. Conclusion: This method has good reproducibility and separation effect.
Name: Filled Column
Specification: 2m * 4mm, 60-80 mesh
Model: Polyethylene glycol filled column/6201 glazed support
No.: 20230510002
*High temperature: 240 ° C
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